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It is important to remember that for the most demanding heat removal requirements, one should always consider introducing a solvent that can be made to boil at the process temperature and pressure, vaporizing that solvent, condensing it, and returning (i.e., re uxing) the condensate to the vessel. This option is often overlooked when designing a heat removal system. There are myriad re ux cooling applications in industrial practice, and an excellent example is the re ux cooling used to remove the heat of polymerization from polystyrene reactors by evaporating and condensing the styrene monomer. The geometry of internal coils needs to be selected carefully because all geometries are not equally effective. The most important geometrical considerations are summarized in Table 14-2. The vessel, vessel internals, and an agitation source are the components of the typical installation. Mechanical agitators (consisting of a drive, a drive shaft, and an impeller) are most often used to

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The population at risk for a given tenure t is the population at risk for t 1, plus Customers who enter the time window with tenure t (that is, those who have tenure t on the left truncation date), minus Customers who leave the time window with tenure t 1 (that is, those who are stopped or censored at the previous tenure).

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impeller size, and proximity of feed to the impeller. Feed component B is usually added to resident component A when component B participates in both reactions. Paul and Treybal (1971) made measurements of the nal yield of one product of a competitive-consecutive reaction as a function of impeller speed in two small (T = 0.15 m and 0.29 m) semibatch reactors, showing how mixing rate affects yield. The data for the 0.29 m-diameter vessel are plotted in Figure 13-35. In the reaction sequence used by Paul and Treybal, A was tyrosine, B was iodine, R was monoiodated tyrosine, and S was diiodated tyrosine. Iodine was fed at a concentration of 2 mol/L into tyrosine at 0.2 mol/L. Canon et al. (1977) simulated the ow, mixing, and reaction in the Paul and Treybal stirred reactor using a Monte Carlo coalescence and dispersion (C-D) method. In this method elements of the uid are simulated by points that move according to the ow pattern in the vessel. These points have mass and composition representing some fraction of the uid in the vessel. The points are caused to mix (coalesce), react, then disperse. The number of points undergoing C-D during each time increment is proportional to a C-D frequency. The local C-D frequency (coalescences/time/site) was found to be related to local turbulence as follows: ICD = 0.1 L2 S

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High-Pressure Autoclave A high-pressure two-phase alkyl phenol reaction was to be scaled up from experimental data collected from sealed rocking bomb bench scale experiments At any given rocking speed, mixing intensity varies with the amount of liquid in the bomb For example, a half-full autoclave provides more mixing intensity than a nearly full one Mixing intensities in the rocking bomb experiments were compared to agitation rates in a stirred autoclave reactor using the surviving drop method Drop sizes were determined as a function of rocking bomb loading and compared to those versus speed in the stirred autoclave Figure 12-40 shows the relationship found between the ll level in the bomb and the agitation speed in the stirred autoclave The laboratory stirred vessel was actually never used for reaction experiments It was simply a scaled-down version of the commercial autoclave geometry and operating conditions.

TABLE 25-1

One of the most useful features of a pivot table is the ability to combine items into groups. You can group items that appear as Row Labels or Column Labels. Excel offers two ways to group items: n Manually: After creating the pivot table, select the items to be grouped and then choose PivotTable Tools Options Group Group Selection. Or, you can right-click and choose Group from the shortcut menu. n Automatically: If the items are numeric (or dates), use the Grouping dialog box to specify how you would like to group the items. Select any item in the Row Labels or Column Labels and then choose PivotTable Tools Options Group Group Selection. Or, you can right-click and choose Group from the shortcut menu. In either case, Excel displays its Grouping dialog box.

More detailed information can be found from some of the sources listed in the references section [1, 2].

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